Submitted by Tim Herzog / Weber State University on Mon, 12/21/2020 - 10:32
Forums

In my senior level inorganic lab, I've tried to incorporate full semester research projects.  Since I love synthesis, I have tended to assign synthetic projects.  Students have learned a lot during these experiences, but there are the obvious challenges of multistep synthetic work in a 3 hour a week lab. I'd like to try to develop projects that are more mechanistic in nature, but am struggling to come up with ideas that are both compelling and achievable.  We will be working in lab this spring with social distancing and some restrictions, but should be able to do all the things we normally do.   All ideas are appreciated!  

Thanks and Happy Holidays.

Tim

Amanda Reig / Ursinus College

Not sure if this is at all the type of thing you might be looking for, but I'm planning to do a version of the experiments linked below, which have lots of directions you could take the project.  I have done the synthesis and identification of the cis/trans via group theory IR in the past with success and will be trying to add the NMR-based mechanism piece this spring.

https://pubs.acs.org/doi/10.1021/ed080p1044

https://static1.squarespace.com/static/5707ede0d210b8708e037a1e/t/58b70…

 

Mon, 12/28/2020 - 18:58 Permalink
Kyle Grice / DePaul University

What about screening conditions/catalysts for a challenging C-C or C-X cross-coupling? In early weeks students could make calibration curves for GC analysis and pick out conditions to try. After the first round, the class compares data and plans a second round of experiments?

Kyle 

Mon, 01/04/2021 - 10:31 Permalink