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Kyle Grice, DePaul University
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Joined: 07/22/2010 - 5:29pm

Silylating NMR tubes

Hi All,

I was looking up techniques to silylate J-Young NMR tubes to reduce the chances of adventiitous water/SiOH groups doing unwanted chemistry. Has anyone done this before and what conditions/reagents did they use? 

Thanks,

Kyle