Synthesis and characterization of 12-tungstosilicic acid - a modification

Submitted by Randall Hicks / Reed College on Mon, 11/15/2010 - 23:25
Description
This lab experiment is an update on the synthesis of the title acid. An account of this synthesis can be found in William Jolly's book, The Synthesis and Characterization of Inorganic Compounds. The synthetic procedure is reliable and was retained. However, I modified some content and added components to extend to a two-week experiment. This lab now covers the synthesis, an acid-base titration with error analysis, and the use of TGA to complement the titration results.

Inorganic Chemistry of Organ Pipes: Composition and Corrosion

Submitted by Catherine Oertel / Oberlin College on Thu, 09/30/2010 - 14:46
Description

This presentation provides an inorganic chemist's perspective on metals used to make organ pipes and their corrosion and conservation.  The slides highlight my own research in this area as well as work being done by other scientists around the world.  The purpose of this learning object is to show students an application of inorganic chemistry that they probably have not encountered before and show an example of how analytical methods of materials chemistry can be used in conservation science.   

Towards "Personalized Solar Energy": An Inexpensive Oxygen-Evolving Catalyst

Submitted by Anne Bentley / Lewis & Clark College on Fri, 08/27/2010 - 15:54
Description

In the two years since this article was published, it has jump-started a large amount of research in the area of cobalt-based catalysts for solar water splitting.  The paper describes the electrochemical synthesis and oxygen-evolution capabilities of a Co-phosphate catalyst under very mild conditions.  The paper can stimulate discussion of many topics found in the inorganic curriculum, including electrochemistry, semiconductor chemistry, transition metal ion complex kinetic trends, and solid state and electrochemical characterization techniques.

Dye-Sensitized Solar Cell 2010

Submitted by Simon Garcia / Kenyon College on Tue, 08/03/2010 - 16:37
Description

In this laboratory experiment, students construct a solar cell from a combination of synthetic and natural materials. It touches on a variety of chemical principles (kinetics, photochemistry, electrochemistry, intermolecular forces, material properties); however, the primary aim is the experience of turning materials into components and then assembling them into a working device. This experiment is unique in that it emphasizes each material's function, and how its properties affect this function. Students can seal these solar cells and take them home afterward.

Teaching General Chemistry: A Materials Science Companion

Submitted by Maggie Geselbracht / Reed College on Mon, 07/26/2010 - 18:15
Description

This book was originally written (full disclosure: I am one of the co-authors) for college teachers as a resource text to encourage and support the incorporation of more solid state and materials chemistry into the general chemistry curriculum.  The Companion, as I refer to it, is filled with background material, demonstrations, laboratory experiments, and end-of-chapter problems that will aid the non-specialist in enriching their teaching with examples from the world of solid state materials.  Although intended for a general chemistry audience, several of the chapters present fairly sophis

Powder Diffraction Crystallography Instructional Materials

Submitted by Barbara Reisner / James Madison University on Mon, 06/28/2010 - 11:03
Description
Brian Toby (Argonne National Labs) has assebled an excellent series of tutorials on using the Rietveld analysis technique for powder diffraction data. Tutorials range from an "Introduction to Crystallography" and "Getting Started with Rietveld" to using the "Le Bail Intensity Extraction" Method to "Advanced Rietveld Techniques."

Introduction to the Synthesis and Properties of Nanoparticles

Submitted by Brian Johnson / St. John's University/College of St. Benedict on Fri, 04/30/2010 - 09:59
Description

This activity leads students through the synthesis of compound nanoparticles and examines how key physical properties such as band gap vary with particle size.  Prior to doing this, students should have some exposure to the structure of solids, band theory, and band gap as a periodic property (see, for example, Lisensky, et al. J Chem.

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