Trap-to-Trap Distillation of Volatile Organic Liquids (Polyhalomethanes)
This lab exercise uses air-stable compounds (polyhalomethanes) to demonstrate trap-to-trap distillation, a technique used to separate air-sensitive compounds. The apparatus (including part numbers from CHEMGLASS) is described. In addition, slush baths are employed, which are a novelty for our Inorganic Laboratory course and a source of amazement for the students. The separation of the compounds (the percentage each compound in each trap) is determined by 1H NMR.