[TaCl2(NMe2)3]2

We're trying to follow the old Chisholm prep from 1981 (http://dx.doi.org/10.1021%2Fic50220a049) and are getting super low yields.  Any words of advice?

Ta(NMe2)5 + 2 TMSCl --> [TaCl2(NMe2)3]2 + 2 TMSNMe2

Adam Johnson / Harvey Mudd College Fri, 07/11/2008 - 13:26
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